Volumetric determination of columbium

Volumetric determination of columbium.

The quantitative determination of columbium based on reduction by amalgamated zin c and reox idation with potassium permanganate has, in general, produced results that lack both accuracy and precision. A study of t he various factors involved indicates that essential conditions requ ire adequate duration of reduction in t he presence of an excess of zinc and a proper concentration of both acid ...

EDWARDS : Volumetric Determination Of Carbon

Volumetric determination of calcium in blood serum.

DETERMINATION OF COLUMBIUM IN ORES BY X-RAY FLUORESCENCE1 JouN S. SrevrNsoN, McGill Uniaersity, Montreal, Quebec. AssrRecr

Analyses for columbium in pyrochlore ores from North Bay, Ontario, have been made successfully by using o-ray fluorescence techniques. rt was necessary to use, as in methods of optical spectroscopy) an internal standard for this work. The choice of a suitable internal standard for a particular metal in a specific mineral association or ore-t).pe requires consideration of the characteristic r-ra...

Volumetric and spectrophotometric determination of oxcarbazepine in tablets.

Two cerimetric procedures are described for the assay of oxcarbazepine (OXC) in bulk drug and in tablets. Titrimetry (method A) is based on the reaction of OXC by a measured excess cerium(IV) sulphate in sulphuric acid medium and the determination of the unreacted oxidant by titration with iron(II) solution using ferroin as indicator. Spectrophotometry (method B) is based on oxidation of OXC by...